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Series 4540 600-1200 mL High Pressure Reactors
Stirred Reactors and Pressure Vessels
High Pressure Reactors, Series 4540 | Parr Instrument Company

 

4540

Model 4544 High Pressure Reactor, 600 mL, Moveable Style Vessel, with heater
lowered, and a 4848 Controller shown with optional Expansion Modules.

Links to documents of interest:
394M Operating Instructions for Series 4540
4540 Sales Literature - Catalog 11

234M Magnetic Drive Operating Instructions
231M Rupture Disc Instructions
230M Safety in the Operation of Reactors & Pressure Vessels
201M Limited Warranty

This series of stirred reactors has been designed for users who need higher operating pressures than the 2000 to 3000 psi offered by the General Purpose Reactors, but do not require the high operating temperatures provided by the Series 4570 High Pressure, High Temperature Reactors. These reactors offer working pressures to 5000 psi (345 bar) at temperatures to 350 °C.

These vessels have been designed with outside dimensions comparable to the Series 4520 and 4530 Reactors so that they can use the same support system, stirrer drive and heater as these popular general purpose models. This provides not only an attractively priced high pressure/moderate temperature system, but also reactors that can be interchanged with the 1 and 2 liter sizes. The thicker walls required for higher operating pressures reduce the volumes of these reactors to 600 and 1200 mL.

These reactors can be used in either the bench top or floor stand mountings. While the 1200 mL reactor is offered as a “bench top model”, it is too tall and too heavy to be handled comfortably on a standard height bench top. It is recommended that the floor stand support option should be selected unless the user has an “adjustable bench top” which will accommodate the overall height of the 1200 mL systems.

 

Series 4540 Pressure Reactor System Specifications
Shaded bar indicates specifications that change within series.
Model No. - Moveable Vessel 4544 4546 4544A 4546A 4544C

4546C

Model No. - Fixed Head 4545 4547 4545A 4547A
Sizes, mL 600 1200 600 1200 600 1200
Maximum Pressure (MAWP) 5000 psi (345 bar)
Maximum Temperature
with PTFE Flat Gasket 350 °C
Vessel Details
Reactor Mounting Bench Top Floor Stand Moveable Cart
Closure Split-Ring (8 Cap Screws)
Valve Connections 1/4" Male NPT
Magnetic Stirrer, Model No. A1120HC6
Maximum Torque 16 Inch-Pounds
Impeller(s), 6-Blade 2 (1.75" dia.)
Pressure Gage, Size 4.5 inches
Range 5,000 psi (345 bar)
Temperature Measurement Thermowell
Cooling Coil Optional
Style Serpentine
Bottom Drain Valve A177VB 1" NPS
Heater Style Calrod
Heater Power, Watts 1000 1500 1000 1500 1000 1500
Stirrer Motor, hp 1/8 1/8 1/8 1/8 1/4 1/4
Electrical Supply
Volts, AC 115 or 230
Maximum Load, amps, 115 / 230 14 / 7
Vessel Dimensions
Inside Diameter, inches 3.25
Inside Depth, inches 4.7 9.8 4.7 9.8 4.7 9.8
Weight of Vessel, pounds 51 57 51 57 51 57
Reactor Dimensions
Width, inches 16.5 20.5 35
Depth, inches 23.5 27.5 18
Height, inches 45.5 56.2 50
Weight, pounds 125 135 175 185 175 185
Spare Parts Kit 4549MA 4549MB 4549MB

Other options available. See Ordering Guide or call for more information.

 

Model 4546C Reactor, 1200 mL, Moveable Head Style,
on a Moveable Cart, and a 4848 Reactor Controller
shown with optional Expansion Modules.

 

1200 mL Fixed Head, and 600 mL Moveable Reaction Vessels.

 

Series 4540 Ordering Guide

The Order No. for the Base System is: 454__-T-SS-M-115-VS.12-2000-4848
A composite identification number to be used when ordering a 4540 Series Reactor can be
developed by combining individual symbols from the separate sections below.

ABase Model
Model No. Size Vessel Style
4544 600 mL Moveable Bench Top
4544A 600 mL Moveable Floor Stand
4544C 600 mL Moveable Cart
4545 600 mL Fixed Head Bench Top
4545A 600 mL Fixed Head Floor Stand
4546 1200 mL Moveable Bench Top
4546A 1200 mL Moveable Floor Stand
4546C 1200 mL Moveable Cart
4547 1200 mL Fixed Head Bench Top
4547A 1200 mL Fixed Head Floor Stand
BGasket / Maximum Temperature
-T PTFE Compression Gasket / 350 °C
CMaterials of Construction
-SS T316 Stainless Steel
-MO Alloy 400
-IN Alloy 600
-HB Alloy B-2
-HC Alloy C-276
-CS Alloy 20
-TI2 Titanium Grade 2
-TI4 Titanium Grade 4
-NI Nickel 200
-ZR Zirconium Grade 702 or 705
DMagnetic Stirrer Drive
-M General Purpose, 16 in-lb
-FMD1 Footless, General Purpose, 16 in.-lb,
EMag. Drive Material of Construction
-No Symbol Same Material As Vessel
-MOC Symbol Indicate Material of Construction
FElectrical Supply
-115 115 VAC
-230 230 VAC
GMotor Option
-VS .12 Variable Speed, 1/8 hp
-VS .25 Variable Speed, 1/4 hp
-XP .25 Explosion Proof, Variable Speed, 1/4 hp
-AM .25 Air Motor, 1/4 hp
HPressure Gage
-3000 3000 psi / 200 bar
-5000 5000 psi / 345 bar
IInternal Cooling Coil
-No Symbol No Coil
-SC Serpentine Coil
JBottom Drain Valve
-No Symbol No Bottom Drain Valve
-BDV Bottom Drain Valve, 1" NPS
KController
-4848 PID Control, Ramp & Soak Programming, Motor Speed Control, and Data logging with Software
-A1925E4 Optional RS485 to USB Cable for 4848 Controller
-4871 Process Controller
L4848 Expansion Modules
-TDM Tachometer Display Module
-MCM Tachometer w/Motor Control Module
-PDM Pressure Display Module
-HTM High Temperature Cut Off Module
-ETLM External Temperature Limit Module
-MTM Motor Torque Module
M4848 Cooling Control: Solenoid Valve Module
-SVM1 115 VAC
-SVM2 230 VAC
NCustom Options (List All Desired)
-AS Anchor Stirrer
-SB Static Catalyst Basket
-CAD Catalyst Addition Device
-BF Baffles
-GE Gas Entrainment Stirrer
-RC Reflux Condenser
-RTC Reflux Take-off Condenser
-ABH Aluminum Block Heater
-WJ Welded Jacket
-SCP Solids Charging Port
OCertifications
-No Symbol No Certification
-ASME ASME Certification
-CE/PED European Community Certification
-CH China Certification
-P Parr Certification
PSpare Parts Kit
-4549MA Spare Parts Kit for 4544-4547
-4549MB Spare Parts Kit for 4544A-4547A, 4544C, 4546C

Stirred Reactors, Series 4540, 600-1200 mL High Pressure Reactors

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Today's Date: 09 September 2010
Parr Instrument Company
211 Fifty Third Street
Moline, Illinois 61265-9984
1-800-872-7720 / (309) 762-7716 FAX (309) 762-9453
Email: parr@parrinst.com