High Temp – High Pressure Reactors, Series 4570-4580

Model 4577 High Temperature/High Pressure Reactor, Floor Stand,
Fixed Head 1000 mL with Heater and Pneumatic Lift.

Links to documents of interest:
397M Operating Instructions for Series 4570
398M Operating Instructions for Series 4580
4570/80 Sales Literature - Catalog 11

234M Magnetic Drive Operating Instructions
231M Rupture Disc Instructions
230M Safety in the Operation of Reactors & Pressure Vessels
201M Limited Warranty

Parr offers a number of different reactors in the 4570 and 4580 Series in a variety of sizes and with different mountings for operating pressures to 5000 psi (345 bar) and temperatures to 500 °C.

4571 - 4572 Reactors
These are 1000 and 1800 mL moveable head reactors mounted in movable carts.

4577 - 4578 Reactors
These are 1000 and 1800 mL fixed head reactors mounted on a floor stand with pneumatic lift.

4575 - 4576A Reactors
These are 500 and 250 mL bench top reactors with 5000 psi (345 bar) and 500 °C ratings. They are available as either moveable or fixed head vessels.

4581 - 4582 Reactors
These 1 gallon (3.75 L) and 1.5 gallon (5.5 L) reactors are designed for 3000 psi (200 bar) maximum pressure with a 500 °C maximum working temperature and mounted on movable carts.

4583 - 4584 Reactors
These are 1 gallon (3.75 L) and 1.5 gallon (5.5 L) fixed head reactors mounted on floor stands with pneumatic lift.

All of these reactors have been designed with suitable valves, fittings and modifications to the vessel itself to operate at the higher temperature and pressure ratings.

Flat, flexible graphite (FG) gaskets are used for temperatures in the higher range to 500 °C. These can be replaced with PTFE gaskets for procedures in which the temperature will not exceed 350 °C. All cart and floor stand models use ceramic fiber heaters to achieve the higher operating temperatures.

Series 4570/80 Pressure Reactor System Specifications
Shaded bar indicates specifications that change within series.
Model No. – Moveable Vessel	4571	4572	4581	4582	4575B	4576B
Model No. – Fixed Head	4577	4578	4583	4584	4575A	4576A
Reactor Mounting	Cart / Floor Stand		Cart / Floor Stand		Bench Top
Sizes, mL	1000	1800	3750	5500	500	250
Maximum Pressure, MAWP	5000 psi (345 bar)		3000 psi (200 bar)		5000 psi (345 bar)
Maximum Temperature
with FG Flat Gasket	500 °C
Vessel Details
Closure (Cap Screws)	Split Ring (12)		Split Ring (16)		Split Ring (8)
Valves Mounted	Head
Valve Connections	1/4" NPT Female
Magnetic Stirrer, Model No.	A1120HC		A1180HC		A1120HC
Maximum Torque	16 Inch-Pounds		60 Inch-Pounds		16 Inch-Pounds
Impeller(s), 6-Blade (4-blade)	2 (2" dia.)		2 (3.5" dia.)		2 (1.38" dia.)
Pressure Gage, Size	4.5 inches
Range	0-5000 psi (345 bar)
Temperature Measurement	Thermowell
Cooling Coil	Included
Style	Serpentine		Serpentine		Single Loop
Bottom Drain Valve	A177VB		A177VB		Custom
Heater Style	Ceramic
Heater Power, Watts	2300	2500	2800		1000
Stirrer Motor, Variable Speed	1/4 hp		1/2 hp		1/8 hp
Electrical Supply
Volts, AC	230		230		115 or 230
Maximum Load, amps, 115 / 230	13	14	15		12 / 6
Vessel Dimensions
Inside Diameter, inches	3.75		5.5		2.5
Inside Depth, inches	6.2	10.5	9.7	15	6.6	3.2
Weight of Moveable Vessel, pounds	70	85	100	130	35	29
Weight of Fixed Vessel, pounds	85	100	120	160	37	31
Reactor Dimensions
Moveable Width x Depth x Height, in.	Cart: 35 x 18 x 50		Cart: 35 x 18 x 50		Bench Top: 17 x 24 x 41
Fixed Width x Depth x Height, in.	Floor Stand: 20 x 33 x 75		Floor Stand: 20 x 33 x 75
Moveable Weight w/Controller, pounds	245	265	325	355	125	120
Fixed Weight w/Controller, pounds	265	285	345	375	127	122
Spare Parts Kit	4579B		4589B		4579D
Other options available. See Ordering Guide or call for more information.

Model 4581 High Temperature/High Pressure Reactor,
with One Gallon Moveable Vessel, and a 4848 Reactor Controller
with optional Expansion Modules

Model 4576A HT/HP Reactor, Fixed Head Bench Top, with
250 mL Vessel

Model 4575B High Pressure/High Temperature 500 mL
Moveable Vessel Assembly.

Series 4570/80 Ordering Guide

The Order No. for the Base System is: 457__ or 458__-FG-M or HD-SS-115 or 230-VS.__-5000-4848
A composite identification number to be used when ordering a 4570 or 4580 Series Reactor
can be developed by combining individual symbols from the separate sections below.

ABase Model
Model	Size	Vessel Style
4571	1000 mL	Moveable Head, Cart
4572	1800 mL	Moveable Head, Cart
4575B	500 mL	Moveable Head, Bench Top
4576B	250 mL	Moveable Head, Bench Top
4575A	500 mL	Fixed Head, Bench Top
4576A	250 mL	Fixed Head, Bench Top
4577	1000 mL	Fixed Head, Floor Stand
4578	1800 mL	Fixed Head, Floor Stand
4581	1.0 Gallon	Moveable Head, Cart
4582	1.5 Gallon	Moveable Head, Cart
4583	1.0 Gallon	Fixed Head, Floor Stand
4584	1.5 Gallon	Fixed Head, Floor Stand

BGasket / Maximum Temperature
-FG	Flexible Graphite Gasket, 500 °C
-T	PTFE Compression Gasket, 350 °C

CMaterials of Construction
-SS	T316 Stainless Steel
-MO	Alloy 400*
-IN	Alloy 600
-HB	Alloy B-2*
-HC	Alloy C-276
-CS	Alloy 20*
-TI2	Titanium Grade 2*
-TI4	Titanium Grade 4*
-ZR	Zirconium Grade 702* or 705*
* Maximum temperature limited.

DMagnetic Stirrer Drive for 4575-76 Only
-M	General Purpose, 16 in-lb
-FMD	Footless, General Purpose, 16 in-lb

EMagnetic Stirrer Drive for 4571-4584 Only
-M	General Purpose , 16 in-lb
-HD	Heavy Duty, 60 in-lb
-XHD	Extra Heavy Duty, 120 in-lb
-FMD1	Footless, 16 in-lb.
-FMD2	Footless, Heavy Duty, 60 in-lb
-FMD3	Footless, Extra Heavy Duty, 120 in-lb

FMag. Drive Material of Construction
-No Symbol	Same Material As Vessel
-MOC Symbol	Indicate Material of Construction

GElectrical Supply
-115	115 VAC (4575-4576 Only)
-230	230 VAC

HMotor Option
-VS .12	Variable Speed, 1/8 hp (4575-4576 Only)
-VS .25	Variable Speed, 1/4 hp
-VS .50*	Variable Speed, 1/2 hp
-XP .25	Explosion Proof Variable Speed, 1/4 hp

-XP .50*	Explosion Proof Variable Speed, 1/2 hp
-AM .25	Air Motor, 1/4 hp (4575-4576 Only)
-AM .50*	Air Motor, 1/2 hp
-GDD	Geared Direct Drive (Fixed Head Unit Only)
* For use with Heavy Duty (HD) Magnetic Stirrer Drive. Only available on 230V systems.

IPressure Gage
-2000	2000 psi / 140 bar
-3000	3000 psi / 200 bar
-5000	5000 psi / 345 bar

JBottom Drain Valve
-No Symbol	No Bottom Drain Valve
-BDV	Bottom Drain Valve (Not available on 250 mL or Bench Top Systems.)

KController
-4848	PID Control, Ramp & Soak Programming, Motor Speed Control, and Data logging with Software
-A1925E4	Optional RS485 to USB Cable for 4848 Controller
-4871	Process Controller

L4848 Expansion Modules
-TDM	Tachometer Display Module
-MCM	Tachometer w/Motor Control Module
-PDM	Pressure Display Module
-HTM	High Temperature Cut Off Module
-ETLM	External Temperature Limit Module
-MTM	Motor Torque Module

M4848 Cooling Control: Solenoid Valve Module
-SVM1	115 VAC
-SVM2	230 VAC

NCustom Options (List All Desired)
-AS	Anchor Stirrer
-SB*	Static Catalyst Basket
-GE	Gas Entrainment Stirrer
-RC	Reflux Condenser
-RTC	Reflux Take-off Condenser
-BF	Baffles
* Not available on 250 mL vessels

OCertifications
-No Symbol	No Certification
-ASME	ASME Certification
-CE/PED	European Community Certification
-CH	China Certification
-P	Parr Certification

PSpare Parts Kit
-4579B	Spare Parts Kit for 4571, 4572, 4577, 4578
-4589B	Spare Parts Kit for 4581, 4582, 4583, 4584
-4579B	Spare Parts Kit for 4575B, 4576B, 4575A, 4576A

Stirred Reactors, Series 4570-4580, High Temperature – High Pressure Reactors

Series 4570-4580 HT/HP Reactors

Today's Date: 09 September 2010
Parr Instrument Company
211 Fifty Third Street
Moline, Illinois 61265-9984
1-800-872-7720 / (309) 762-7716 FAX (309) 762-9453
Email: parr@parrinst.com