Fixed Head Reactors
Parr offers most of its laboratory reactors in a fixed head design. This includes all reactors with volumes from 25 mL to 20 liters. In these reactors the head of the vessel may remain fixed in the reactor support stand. All attachments to the head: gas and liquid feed and discharge lines, cooling water, vapor take-off and condenser, thermocouple and any electrical leads can remain permanently in place. The reactor is opened by simply removing the split-ring and lowering the cylinder away from the head, leaving all of the attachments undisturbed. If desired the complete vessel assembly can be removed from the head support plate.
The support frames for fixed head reactors vary based on the sizes and weights of the vessels.
- For vessels with volumes of 25 mL to 600 mL, the cylinder may be lowered and removed manually by the operator.
- Vessels with volumes of 1 to 2 liters include a manual lift mechanism to raise or lower the cylinder.
- Vessels with volumes greater than two liters or where weight dictates include a pneumatic cylinder lift mechanism.
Moveable Vessel Reactors
As an alternate to the fixed head designs described in the previous section, all Parr reactors can be furnished in designs which allow the entire vessel to be removed as a complete assembly from the support stand allowing for charging, product recovery, and cleaning. In the smaller and mid-sized models the entire vessel is simply lifted out of the heater by hand. In the larger models, the vessel can be opened and closed with the cylinder remaining in the heater, but the head must be lifted off manually. In the largest (10 L and 20 L) models a chain hoist is provided for lifting the heavier head and cylinder.
These moveable reactors will be attractive to users that intend to operate fairly simple batch systems rather than continuous flow arrangements, and that want to be able to remove the vessel for product recovery, charging or cleaning. They will also appeal to those that need to prepare the vessel in a special atmosphere, or want to clean the cylinder and stirrer at a site away from the reactor stand and heater. There is also the added advantage of being less expensive than the fixed head models since they do not require the more elaborate head or the cylinder and heater lift mechanism.
Accessories
4878 Automated Liquid Sampler
Catalyst Addition Devices
Catalyst Baskets
Catalyst Loading Toolkit
Catalyst Testing System
Condensers
Coned Pressure Fittings
Continuous Bulk-Solids Feeder
Controllers
Cooling Coils
Equipment for Use in Potentially Ignitable Atmospheres
External Valves and Fittings
Gas Measurement Systems
--Intermediate Supply Tanks
--Mass Flow
--High Pressure Gas Burettes
Heaters
Insulated Electrical Glands
Liners
Liquids Charging Systems
--Liquid Metering Pumps
--Liquid Charging Pipettes
Magnetic Drives
Motors and Drives
Pressure Gages
Pressure Hose
Safety Rupture Discs
Sample Collection Vessel
Service Fixtures
Solids/Slurry Addition Devices
Spare Parts Kits
Split-Ring Closures
--Stirrer Options
--Gas Entrainment Impellers
Temperature Limits
Thermocouples
Valves and Fittings
--Bottom Drain Valves
--Manual Control Valves for Compressed Gas Tanks
--Pressure Relief Valves
--Safety Check Valves
Windows