Catalyst baskets can be provided for holding a supported catalyst so that it will not be destroyed or changed by the stirring action of the impeller. These can be installed in reactors with volumes ranging from 300 to 2000 mL. Two interchangeable styles are available. Special heads, internal cooling coils, thermowells and dip tubes are required to provide clear space in the vessel for these baskets.
Catalyst Basket Assemblies | ||||
Reactor | Reactor Volume | Basket Style | Catalyst Volume (cm3) |
|
4561* | 300 | Static | 40 | |
4562* | 450 | Static | 40 | |
4563* | 600 | Static | 40 | |
4566* | 300 | Static | 40 | |
4567* | 450 | Static | 40 | |
4568* | 600 | Static | 40 | |
4521/31 | 1000 | Static | 150 | |
4521/31 | 1000 | Dynamic | 150 | |
4522/32** | 2000 | Static | 150 | |
4522/32* | 2000 | Dynamic | 150 | |
4544* | 600 | Static | 40 | |
4545* | 600 | Static | 40 | |
4546* | 1200 | Static | 40 | |
4547* | 1200 | Static | 40 | |
4548* | 1200 | Static | 40 | |
4571/73 | 1000 | Static | 150 | |
4571/73 | 1000 | Dynamic | 150 | |
4572/74* | 1800 | Static | 150 | |
4572/74* | 1800 | Dynamic | 150 | |
4575 | 500 | Static | 40 | |
*May require special inlet tube and thermowell |
The Static Design
In the static design the mesh basket holding the catalyst remains stationary while impellers on the stirring shaft and baffles outside of the basket direct the flow of reactants over the surface of the contained catalyst. A unique gas entrainment impeller provides a uniform flow of both gas and liquid over the fixed catalyst bed held within the annular basket. The Parr design for these baskets includes a rigid bottom support which permits high speed stirring without excessive vibration. Cooling coils, internal temperature measurements and liquid and gas sampling operations can be continued as usual without interference from the installed catalyst basket.
The Dynamic Design
In the dynamic design the catalyst is held in an annular shaped, mesh basket which is attached to the stirrer drive in place of the stirring shaft. The rotating basket then serves as an impeller for stirring the reactants. Fixed baffles and coaxial impellers ensure good circulation over the surface of the contained catalyst. The dynamic baskets are available for reactors with volumes of 1000, 1800 and 2000 mL. Dynamic baskets must be installed in reactors equipped with at least 1/4 hp motors to ensure that sufficient stirrer torque and speeds are available for proper operation. Dynamic baskets are interchangeable with static baskets in 1 liter and larger vessels.
Accessories
4878 Automated Liquid Sampler
Catalyst Addition Devices
Catalyst Baskets
Catalyst Loading Toolkit
Catalyst Testing System
Condensers
Coned Pressure Fittings
Continuous Bulk-Solids Feeder
Controllers
Cooling Coils
Equipment for Use in Potentially Ignitable Atmospheres
External Valves and Fittings
Gas Measurement Systems
--Intermediate Supply Tanks
--Mass Flow
--High Pressure Gas Burettes
Heaters
Insulated Electrical Glands
Liners
Liquids Charging Systems
--Liquid Metering Pumps
--Liquid Charging Pipettes
Magnetic Drives
Motors and Drives
Pressure Gages
Pressure Hose
Safety Rupture Discs
Sample Collection Vessel
Service Fixtures
Solids/Slurry Addition Devices
Spare Parts Kits
Split-Ring Closures
--Stirrer Options
--Gas Entrainment Impellers
Temperature Limits
Thermocouples
Valves and Fittings
--Bottom Drain Valves
--Manual Control Valves for Compressed Gas Tanks
--Pressure Relief Valves
--Safety Check Valves
Windows